HPLC-MS Determination of Iopromide and Iopamidol in Waters Using On-line Preconcentration in Porous Graphite Columns

Authors

  • J. Kokšal Ohře River Basin, Department of Water Laboratories, Teplice
  • R. Beranová Ohře River Basin, Department of Water Laboratories, Teplice

Keywords:

iopromid, iopamidol, LC-MS/MS determination, on-line preconcentration, water analysis

Abstract

Determination of Iopromide and Iopamidole in surface and waste waters was developed. A porous graphitic carbon sorbent was used for pre-concentration and separation of analytes, in combination with tandem mass spectrometry as detection technique. The method was validated and applied in routine analyses. Its characteristics such as repeatability, limits of detection and determination are presented together with evaluation of matrix effects. The working range was 20–1000 ng L–1, limit of determination 20 ng L–1 and expanded uncertainty 30 %.

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Published

2014-10-15

How to Cite

Kokšal, J., & Beranová, R. (2014). HPLC-MS Determination of Iopromide and Iopamidol in Waters Using On-line Preconcentration in Porous Graphite Columns. Chemické Listy, 108(10), 976–979. Retrieved from http://w-ww.chemicke-listy.cz/ojs3/index.php/chemicke-listy/article/view/453

Issue

Vol. 108 No. 10 (2014)

Section

Articles